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Home  /  Laboratory Instruments  / 
Hydrothermal-Autoclave Chemical Reactor-with-PPL-Chamber

Hydrothermal Autoclave Reactor with PTFE Chamber

Category: Laboratory Instruments
Tags: Chemical Reactor .Laboratory Chemical Reactor., Hydrothermal Autoclave Reactor, lab Instrument /Chemical reactor
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Description

These are the Stainless Steel Hydrothermal Autoclave Reactor + PTFE Chamber Synthesis 10ml, 25ml, 50ml,100ml, 200ml.

Hydrothermal synthesis reactor is used in catalysis, crystal, polymer, and other experiments, it adopts the external heating mode, to reduce the size, and is suitable for several reaction kettles working at the same time and same reaction temperature (for example, put several reactors inside the oven for heating), special models can be customized.

Hydrothermal synthesis reactor, also known as digestion, pressure melting bombs, hydrothermal synthesis reactor, high temperature, and pressure digestion vessels, PTFE high-pressure tank is in a certain temperature and pressure conditions, certain synthetic chemicals supplied reactor.

It is widely used in new materials, energy, environmental engineering, and other fields of scientific research and experiments in university teaching, scientific research units commonly used small reactors.

Main Indicators of Autoclave Reactors 

  • Operating temperature: 220℃
  • Working pressure: 3MPa (gauge)
  • Heating, and cooling rate: 5 ℃ / min

Features of Autoclave Reactor:

1. To dissolve the refractory material and to pretreat the samples in atomic absorption spectrometry and plasma emission analysis, etc.
2. This type of hydrothermal synthesis reactor is most suitable for small-dose synthetic reactions, to rapidly dissolve the refractory material under the reactor’s inner strong acid or strong base and high temperature & high-pressure airtight environment.
3. Todo sample preparation in the gas phase, liquid phase, plasma mass spectrometry, atomic absorption, atomic fluorescence spectrum, and chemical analysis method.
4. Is an ideal instrument to dissolve samples when you measure trace elements and trace elements.
5. Could be used in the measurement of lead, copper, cadmium, zinc, calcium, manganese, iron, mercury, and other heavy metals. Also can be used as a reaction vessel that has high-temperature resistance, high-pressure resistance, and corrosion prevention.
6. Is suitable for organic synthesis, hydrothermal synthesis, crystal growth or sample digestion & extraction, etc.
7. In sample pretreatment dissolve heavy metals, pesticide residues, food, silt, rare earth, aquatic products, organic matter, etc.

Advantages:
  1. High-temperature resistance: Teflon material actual measuring operating temp. is higher than 220℃, advise safe operating temp. ≤ 220℃. PTFE material actual measuring operating temp. is higher than 220℃, advise safe operating temp. ≤ 220℃.
  2. Low-temperature resistance: -196℃ could keep 5%.
  3. Ultra corrosion resistance: resistant to strong acid, strong base, aqua regia, and all kinds of organic solvents.
  4. Insulation resistance: dielectric properties have nothing to do with temperature and frequency.
  5. High lubrication: the friction coefficient of solid materials is the lowest.
  6. No adhesion: don’t adhere to any material, self-lubricity is strong, and the friction coefficient of solid materials is 0.04.
  7. Nonhazardous: is physiologically inert, can be embedded in the human body, has strong aging resistance, and guarantees hydrothermal synthesis reactor long service life.
  8. Anti-pollution: the baseline value of the metallic element is low, with lead content < 10-11g/ml, and uranium content < 10-12g/ml.
  9. Leakproof: falling from a 1.2m high place, hydrothermal synthesis reactor body is no fracture, reactor lid is not loose, no break and leakage phenomenon.

Methods of operation

  • The reaction means and the reactor body, and to ensure the feeding coefficient is less than 0.8.
  • When the Department of Corrosive Reaction when you want to put a PTFE bush, can only be assured the kettle body is from corrosion.
  • A hydrothermal synthesis reactor will be placed on the heater, in accordance with the provisions of the heating rate of heating to the desired reaction temperature (less than the required safety temperature).
  • Completion of the reaction will be when it’s cool, but also in strict accordance with the provisions of the cooling rate operation, to facilitate the safety and reactor life.
  • When confirmation of intra-abdominal temperature below the boiling point solvent reaction system can only open the tank lid after a follow-up operation.
  • Hydrothermal synthesis reactor each time after use to clean, to avoid corrosion.
  • Kettle body, and kettle lid seal line to pay particular attention to cleaning and prevent damage to the bumps.

Note: All the sizes are not in our ready-stock products. Some sizes are ready to stock. After confirmation of the order, we can import from China within 30 days.

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